Synthesis and Characterization of (Mesitylene)tricarbonylmol

A detailed Summary of Synthesis and Characterization of (Mesitylene)tricarbonylmol

Abstract: (Mesitylene)tricarbonylmolybdenum and (chlorobenzene)tricarbonylmolybdenum were synthesized each by different methods. (mesitylene)tricarbonylmolybdenum was produced by a direct method under harsh conditions. (Chlorobenzene)tricarbonylmolybdenum was made by an indirect method under mild conditions.

The transition metals chromium, tungsten, and molybdenum commonly form complexes with benzene rings. The metal forms a bond with the six electrons in the ? system of the benzene ring. In this experiment two of such molybdenum complexes are synthesized: (mesitylene)tricarbonylmolybdenum and (chlorobenzene)tricarbonylmolybdenum shown in figure 1.

Figure 1. (mesitylene)tricarbonylmolybdenum (a) and (chlorobenzene)tricarbonylmolybdenum (b)

Two common methods for the synthesis of these tricarbonylmolybdenum complexes are used in the experiment. Method 1 is used to synthesize (mesitylene)tricarbonylmolybdenum and method 2 is used to make (chlorobenzene)tricarbonylmolybdenum. Method 1, the direct method, involves the heating of hexacarbonylmolybdenum with excess mesitylene. This method requires high reaction temperatures which can result in the decompo

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Abstract Mesitylenetricarbonylmolybdenum, Carbonyl C-O, FT-IR KBr, Mesitylenetricarbonylmolybdenum1 Hexacarbonylmolybdenum, Dr Pearsons, Chlorobenzenetricarbonylmolybdenum2 Tricabonyltrispyridinemolybdenum, Discussion Method, IR NMR, Aldrich Pyridine, Unreacted MoCO6, ir spectrum, method 2, method 1, prepared using, ml added, wavenumber cm-1, mesitylenetricarbonylmolybdenum chlorobenzenetricarbonylmolybdenum, nmr spectrum, solution filtered, shown figure, table 1 ir, lab table 3, figure 3 hydrogen, spectrum mesitylenetricarbonylmolybdenum table, table 3 ir,

Approximate Word count = 1398
Approximate Pages = 6 (250 words per page double spaced)

Category: Science

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